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10. 11. 12. Ku•cera, B. Ann. Phys. 11:529 (1903). , Chem. Listy 16:256 (1992) Philos. Mag. J. Sci. 45:303 (1923). , Polarography, Vol. Y. 1952. , Z. Phys. Chem. 202:302 (1953). Kemula M. and Coworbers, Bull. , Pol. Sci. Cl. 111 7:73 (1959). , Z. Electrochem. 44:831 (1938). , Advances in analytical Chemistry and Instrumentation, Vol. 2, Wiley Int. Y. (1963) p. 123. B. and White. , Z. Electrochem. 59:666 (1955). , Anal. Chem. 30:1576 (1958). S. and Coworbers, Abel. Chem. 37:1446 (1965). Lind quist, J.
It is to be noted that at the foot of the currentvoltage curve, or polarographic “wave”, and at the limiting current plateau, the dropping electrode behaves is accordance with the definition of a “polarized” electrode. That is to say, the potential applied to it may be altered at will within these regions without sifnificantly altering the current flow. On the rising part of the wave, the current changes considerably for only a small variation in applied potential and the DME is said to be “depolarized”.
Considering the solvent power, an electrochemical solvent must be able to dissolve a wide range of substances at acceptable concentrations. 1 M, while the electroactive material must form approximately millimolar solution for application of the various electroanalytical techniques or greater for preparative electrolyses. Tetra alkyl ammonium perchlorates, hexafluoro phosphates and tetra fluoroborates generally exhibit the most satisfactory solubility as electrolytes in organic solvents. As a matter of fact chemical inertness of the solvent is an important aspect to be considered.
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